TA Instruments

AR1760-0001f

15/03/2013 16:29:59

Sample name	DI 40 mm AL P100
Sample notes	 
Experiment notes	DI Deionised water, 40 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1760
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 16:29:59

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC AL plate with studs
Geometry notes	Standard ETC AL parallel plate with studs
Geometry material	Aluminum
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	2.056 micro N.m.s^2
Geometry compliance	3.130E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	26500 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	1
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.01 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0000	6.400	80.519	10000	20.0	6.154	32.000	26.25	8.000	3.281	25070	5.6855	391.8	7.1068	710.68	3.411E-3	0.0	0.5
2.0000	9.900	13.072	10000	20.0	6.150	33.000	4.261	12.38	0.3443	25060	13.3703	163.6	16.713	1671.3	3.411E-3	0.0	0.6
3.0000	15.48	24.434	10000	20.0	6.150	34.000	7.964	19.35	0.4115	25060	26.9104	66.90	33.638	3363.8	3.411E-3	0.1	0.6
4.0000	18.43	32.149	10000	20.0	6.150	35.000	10.48	23.03	0.4550	25060	40.8442	47.24	51.055	5105.5	3.411E-3	0.1	0.6
5.0000	24.68	50.521	10000	20.0	6.149	36.000	16.47	30.85	0.5338	25050	67.5907	26.33	84.488	8448.8	3.411E-3	0.1	0.6
6.0200	31.59	75.666	10000	20.0	6.151	37.020	24.66	39.49	0.6246	25060	106.9420	16.07	133.68	13368	3.411E-3	0.1	0.6
7.0000	34.03	85.241	10000	20.0	6.147	38.000	27.78	42.54	0.6531	25040	126.3190	13.84	157.90	15790	3.411E-3	0.1	0.6
8.0160	39.30	106.64	10000	20.0	6.145	39.016	34.76	49.13	0.7075	25040	184.8010	10.37	231.00	23100	3.411E-3	0.1	0.7
9.0000	46.03	139.79	10000	20.0	6.135	40.000	45.56	57.54	0.7918	25000	223.1790	7.549	278.97	27897	3.411E-3	0.2	0.7
10.000	50.96	166.96	10000	20.0	6.130	41.000	54.42	63.70	0.8544	24970	274.7880	6.156	343.49	34349	3.411E-3	0.2	0.7
11.000	55.72	192.61	10000	20.0	6.127	42.000	62.78	69.66	0.9013	24960	326.0730	5.145	407.59	40759	3.411E-3	0.2	0.7
12.000	60.10	220.84	10000	20.0	6.120	43.000	71.98	75.12	0.9582	24940	379.8680	4.419	474.84	47484	3.411E-3	0.2	0.7
13.000	64.40	248.00	10000	20.0	6.117	44.000	80.84	80.50	1.004	24920	434.6930	3.846	543.37	54337	3.411E-3	0.2	0.7
14.000	69.14	282.24	10000	20.0	6.111	45.000	92.00	86.43	1.064	24900	498.5590	3.333	623.20	62320	3.411E-3	0.2	0.8
15.000	75.68	331.40	10000	20.0	6.097	46.000	108.0	94.60	1.142	24840	595.0110	2.776	743.76	74376	3.411E-3	0.3	0.8
16.000	79.92	366.62	10000	20.0	6.091	47.000	119.5	99.90	1.196	24820	664.4370	2.487	830.55	83055	3.411E-3	0.3	0.8
17.000	84.52	405.22	10000	20.0	6.084	48.000	132.1	105.6	1.250	24790	740.5120	2.221	925.64	92564	3.411E-3	0.3	0.8
18.000	90.97	463.77	10000	20.0	6.068	49.000	151.2	113.7	1.329	24720	855.2790	1.912	1069.1	1.0691E5	3.411E-3	0.3	0.8
19.000	95.02	504.71	10000	20.0	6.059	50.000	164.5	118.8	1.385	24690	931.7320	1.750	1164.7	1.1647E5	3.411E-3	0.3	0.8
20.000	99.39	545.35	10000	20.0	6.049	51.000	177.8	124.2	1.431	24640	1021.3100	1.597	1276.6	1.2766E5	3.411E-3	0.3	0.9
21.000	105.8	616.32	10000	20.0	6.027	52.000	200.9	132.3	1.519	24560	1153.0800	1.404	1441.4	1.4414E5	3.411E-3	0.4	0.9
22.000	109.9	659.43	10000	20.0	6.015	53.000	214.9	137.4	1.565	24510	1242.6200	1.299	1553.3	1.5533E5	3.411E-3	0.4	0.9
23.008	114.2	711.53	10000	20.0	5.991	54.008	231.9	142.8	1.624	24410	1343.4600	1.197	1679.3	1.6793E5	3.411E-3	0.4	0.9
23.996	120.6	792.67	10000	20.0	5.975	54.996	258.4	150.8	1.713	24340	1495.3900	1.071	1869.2	1.8692E5	3.411E-3	0.4	0.9
25.000	124.7	847.48	10000	20.0	5.961	56.000	276.2	155.9	1.772	24290	1598.0601	0.9991	1997.6	1.9976E5	3.411E-3	0.4	0.9
26.000	129.0	903.05	10000	20.0	5.940	57.000	294.3	161.3	1.825	24200	1710.7700	0.9301	2138.5	2.1385E5	3.411E-3	0.4	1.0
27.024	135.4	992.20	10000	20.0	5.913	58.024	323.4	169.3	1.910	24090	1881.6200	0.8405	2352.0	2.3520E5	3.411E-3	0.5	1.0
28.000	139.5	1046.7	10000	20.0	5.892	59.000	341.2	174.4	1.956	24010	1996.0900	0.7890	2495.1	2.4951E5	3.411E-3	0.5	1.0
29.000	143.6	1114.1	10000	20.0	5.882	60.000	363.1	179.5	2.023	23970	2118.3000	0.7436	2647.9	2.6479E5	3.411E-3	0.5	1.0
30.000	150.0	1207.1	10000	20.0	5.834	61.000	393.5	187.5	2.098	23770	2305.4299	0.6759	2881.8	2.8818E5	3.411E-3	0.5	1.0
31.000	154.2	1269.1	10000	20.0	5.831	62.000	413.7	192.7	2.147	23760	2433.3601	0.6397	3041.7	3.0417E5	3.411E-3	0.5	1.0
32.000	158.2	1342.5	10000	20.0	5.794	63.000	437.6	197.8	2.212	23610	2636.3301	0.6034	3295.4	3.2954E5	3.411E-3	0.5	1.1
33.016	164.6	1445.6	10000	20.0	5.771	64.016	471.2	205.8	2.290	23510	2773.7100	0.5551	3467.1	3.4671E5	3.411E-3	0.6	1.1
34.012	168.8	1522.7	10000	20.0	5.742	65.012	496.3	211.0	2.353	23400	2913.6001	0.5256	3642.0	3.6420E5	3.411E-3	0.6	1.1
35.000	174.9	1625.2	10000	20.0	5.708	66.000	529.7	218.6	2.424	23260	3128.2200	0.4868	3910.3	3.9103E5	3.411E-3	0.6	1.1
36.000	179.1	1703.6	10000	20.0	5.676	67.000	555.3	223.9	2.480	23130	3278.7000	0.4615	4098.4	4.0984E5	3.411E-3	0.6	1.1
37.000	183.3	1785.5	10000	20.0	5.664	68.000	582.0	229.1	2.541	23080	3430.3401	0.4398	4287.9	4.2879E5	3.411E-3	0.6	1.1
38.000	189.3	1894.2	10000	20.0	5.634	69.000	617.4	236.6	2.609	22960	3657.5400	0.4101	4571.9	4.5719E5	3.411E-3	0.6	1.2
39.000	193.4	1976.1	10000	20.0	5.589	70.000	644.1	241.8	2.664	22770	3821.7800	0.3895	4777.2	4.7772E5	3.411E-3	0.7	1.2
40.016	199.7	2075.5	10000	20.0	5.548	71.016	676.5	249.6	2.711	22600	4068.1399	0.3629	5085.2	5.0852E5	3.411E-3	0.7	1.2
41.000	203.7	2178.1	10000	20.0	5.528	72.000	710.0	254.6	2.789	22520	4233.2402	0.3475	5291.6	5.2916E5	3.411E-3	0.7	1.2
42.024	209.9	2300.8	10000	20.0	5.479	73.024	749.9	262.4	2.858	22320	4498.1499	0.3242	5622.7	5.6227E5	3.411E-3	0.7	1.2
43.000	214.1	2385.0	10000	20.0	5.437	74.000	777.4	267.6	2.905	22150	4674.1299	0.3094	5842.7	5.8427E5	3.411E-3	0.7	1.2
43.996	218.1	2479.7	10000	20.0	5.432	74.996	808.3	272.7	2.964	22130	4850.8101	0.2977	6063.5	6.0635E5	3.411E-3	0.7	1.2
45.000	224.3	2608.6	10000	20.0	5.372	76.000	850.3	280.4	3.033	21890	5128.5000	0.2784	6410.6	6.4106E5	3.411E-3	0.8	1.3
46.016	228.4	2684.2	10000	20.0	5.337	77.016	874.9	285.5	3.065	21750	5317.9800	0.2668	6647.5	6.6475E5	3.411E-3	0.8	1.3
47.000	234.5	2831.6	10000	20.0	5.291	78.000	923.0	293.1	3.149	21560	5601.6001	0.2510	7002.0	7.0020E5	3.411E-3	0.8	1.3
48.000	238.5	2920.2	10000	20.0	5.262	79.000	951.9	298.1	3.193	21440	5798.0698	0.2412	7247.6	7.2476E5	3.411E-3	0.8	1.3
49.000	242.7	3020.1	10000	20.0	5.232	80.000	984.4	303.3	3.245	21320	5999.0400	0.2317	7498.8	7.4988E5	3.411E-3	0.8	1.3
50.000	248.8	3164.6	10000	20.0	5.165	81.000	1032	311.0	3.317	21040	6301.8599	0.2176	7877.3	7.8773E5	3.411E-3	0.8	1.4
51.000	252.8	3226.1	10000	20.0	5.093	82.000	1052	316.0	3.328	20750	6509.9302	0.2078	8137.4	8.1374E5	3.411E-3	0.9	1.4
51.996	259.0	3398.7	10000	20.0	5.064	82.996	1108	323.8	3.421	20630	6833.7500	0.1968	8542.2	8.5422E5	3.411E-3	0.9	1.4
53.000	263.1	3493.2	10000	20.0	5.027	84.000	1139	328.8	3.462	20480	7047.3799	0.1894	8809.2	8.8092E5	3.411E-3	0.9	1.4
54.000	269.1	3640.8	10000	20.0	4.969	85.000	1187	336.4	3.528	20240	7374.0098	0.1789	9217.5	9.2175E5	3.411E-3	0.9	1.4
55.000	273.2	3745.8	10000	20.0	4.923	86.000	1221	341.6	3.575	20060	7601.0200	0.1719	9501.3	9.5013E5	3.411E-3	0.9	1.4
55.996	277.3	3864.8	10000	20.0	4.879	86.996	1260	346.7	3.634	19880	7827.9600	0.1654	9785.0	9.7850E5	3.411E-3	0.9	1.4
57.052	283.3	4084.0	10000	20.0	4.859	88.052	1331	354.2	3.759	19800	8168.2700	0.1578	10210	1.0210E6	3.411E-3	1.0	1.5
58.012	287.5	4147.7	10000	20.0	4.797	89.012	1352	359.3	3.762	19550	8407.8896	0.1514	10510	1.0510E6	3.411E-3	1.0	1.5
59.004	293.6	4339.8	10000	20.0	4.784	90.004	1415	367.0	3.855	19490	8777.1602	0.1447	10971	1.0971E6	3.411E-3	1.0	1.5
60.020	297.6	4426.5	10000	20.0	4.678	91.020	1443	372.0	3.879	19060	9006.6797	0.1377	11258	1.1258E6	3.411E-3	1.0	1.5

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

0.99600	300.0	4516.6	10000	20.0	4.656	91.996	1472	375.0	3.926	18970	277.2290	0.1349	346.54	34654	3.411E-3	0.0	1.5
1.9960	300.0	4538.8	10000	20.0	4.697	92.996	1479	375.0	3.945	19140	524.5960	0.1361	655.75	65575	3.411E-3	0.0	1.5
2.9960	300.0	4504.7	10000	20.0	4.656	93.996	1468	375.0	3.915	18970	903.3440	0.1349	1129.2	1.1292E5	3.411E-3	0.0	1.6
3.9960	300.0	4519.8	10000	20.0	4.695	94.996	1473	375.0	3.929	19130	1153.1300	0.1360	1441.4	1.4414E5	3.411E-3	0.1	1.6
4.9960	300.0	4527.9	10000	20.0	4.686	95.996	1476	375.0	3.936	19090	1404.3800	0.1358	1755.5	1.7555E5	3.411E-3	0.1	1.6
5.9960	300.0	4505.6	10000	20.0	4.649	96.996	1469	375.0	3.916	18940	1781.3700	0.1347	2226.7	2.2267E5	3.411E-3	0.1	1.6
6.9960	300.0	4524.7	10000	20.0	4.652	97.996	1475	375.0	3.933	18960	2033.9100	0.1348	2542.4	2.5424E5	3.411E-3	0.1	1.6
8.0000	300.0	4515.1	10000	20.0	4.653	99.000	1472	375.0	3.925	18960	2409.7500	0.1348	3012.2	3.0122E5	3.411E-3	0.1	1.7
8.9960	300.0	4523.1	10000	20.0	4.661	99.996	1474	375.0	3.931	18990	2662.2900	0.1350	3327.9	3.3279E5	3.411E-3	0.1	1.7
9.9960	300.0	4499.4	10000	20.0	4.613	100.996	1467	375.0	3.911	18800	2912.5300	0.1337	3640.7	3.6407E5	3.411E-3	0.2	1.7
11.000	300.0	4558.9	10000	20.0	4.730	102.000	1486	375.0	3.963	19270	3289.3899	0.1370	4111.7	4.1117E5	3.411E-3	0.2	1.7
11.996	300.0	4572.5	10000	20.0	4.719	102.996	1490	375.0	3.975	19230	3540.6899	0.1368	4425.9	4.4259E5	3.411E-3	0.2	1.7
12.996	300.0	4519.0	10000	20.0	4.658	103.996	1473	375.0	3.928	18980	3918.9900	0.1350	4898.7	4.8987E5	3.411E-3	0.2	1.7
13.996	300.0	4523.7	10000	20.0	4.636	104.996	1474	375.0	3.932	18890	4169.0498	0.1344	5211.3	5.2113E5	3.411E-3	0.2	1.7
14.996	300.0	4530.0	10000	20.0	4.694	105.996	1477	375.0	3.938	19120	4421.5098	0.1360	5526.9	5.5269E5	3.411E-3	0.2	1.8
15.996	300.0	4484.7	10000	20.0	4.640	106.996	1462	375.0	3.898	18910	4797.3799	0.1344	5996.7	5.9967E5	3.411E-3	0.3	1.8
16.996	300.0	4497.9	10000	20.0	4.715	107.996	1466	375.0	3.909	19210	5049.9702	0.1366	6312.5	6.3125E5	3.411E-3	0.3	1.8
17.996	300.0	4502.9	10000	20.0	4.671	108.996	1468	375.0	3.914	19030	5299.9902	0.1353	6625.0	6.6250E5	3.411E-3	0.3	1.8
18.996	300.0	4500.2	10000	20.0	4.645	109.996	1467	375.0	3.912	18920	5677.1201	0.1346	7096.4	7.0964E5	3.411E-3	0.3	1.8
20.000	300.0	4500.0	10000	20.0	4.637	111.000	1467	375.0	3.911	18890	5928.2202	0.1343	7410.3	7.4103E5	3.411E-3	0.3	1.9
21.012	300.0	4514.9	10000	20.0	4.673	112.012	1472	375.0	3.924	19040	6305.1899	0.1354	7881.5	7.8815E5	3.411E-3	0.4	1.9
22.072	300.0	4495.7	10000	20.0	4.640	113.072	1465	375.0	3.908	18910	6556.7300	0.1344	8195.9	8.1959E5	3.411E-3	0.4	1.9
22.996	300.0	4487.5	10000	20.0	4.668	113.996	1463	375.0	3.901	19020	6808.1001	0.1353	8510.1	8.5101E5	3.411E-3	0.4	1.9
24.052	300.0	4472.6	10000	20.0	4.630	115.052	1458	375.0	3.888	18860	7186.9102	0.1342	8983.6	8.9836E5	3.411E-3	0.4	1.9
25.000	300.0	4530.8	10000	20.0	4.656	116.000	1477	375.0	3.938	18970	7436.3301	0.1349	9295.4	9.2954E5	3.411E-3	0.4	1.9
26.000	300.0	4529.1	10000	20.0	4.678	117.000	1476	375.0	3.937	19060	7814.4702	0.1355	9768.1	9.7681E5	3.411E-3	0.4	2.0
27.012	300.0	4557.3	10000	20.0	4.658	118.012	1485	375.0	3.961	18980	8064.6899	0.1350	10081	1.0081E6	3.411E-3	0.5	2.0
27.996	300.0	4549.0	10000	20.0	4.681	118.996	1483	375.0	3.954	19070	8318.7002	0.1356	10398	1.0398E6	3.411E-3	0.5	2.0
28.996	300.0	4497.3	10000	20.0	4.647	119.996	1466	375.0	3.909	18940	8692.9004	0.1346	10866	1.0866E6	3.411E-3	0.5	2.0
29.996	300.0	4503.3	10000	20.0	4.675	120.996	1468	375.0	3.914	19050	8944.1602	0.1354	11180	1.1180E6	3.411E-3	0.5	2.0
30.996	300.0	4525.0	10000	20.0	4.659	121.996	1475	375.0	3.933	18980	9195.5098	0.1350	11494	1.1494E6	3.411E-3	0.5	2.0
31.996	300.0	4497.0	10000	20.0	4.661	122.996	1466	375.0	3.909	18990	9572.5898	0.1351	11966	1.1966E6	3.411E-3	0.5	2.0
32.996	300.0	4529.1	10000	20.0	4.654	123.996	1476	375.0	3.937	18960	9823.8203	0.1349	12280	1.2280E6	3.411E-3	0.5	2.1
33.996	300.0	4522.3	10000	20.0	4.658	124.996	1474	375.0	3.931	18980	10202.200	0.1350	12753	1.2753E6	3.411E-3	0.6	2.1
35.000	300.0	4501.9	10000	20.0	4.645	126.000	1467	375.0	3.913	18930	10452.500	0.1346	13066	1.3066E6	3.411E-3	0.6	2.1
35.996	300.0	4492.1	10000	20.0	4.640	126.996	1464	375.0	3.904	18900	10703.600	0.1344	13380	1.3380E6	3.411E-3	0.6	2.1
36.996	300.0	4491.8	10000	20.0	4.653	127.996	1464	375.0	3.904	18960	11080.500	0.1348	13851	1.3851E6	3.411E-3	0.6	2.1
37.996	300.0	4508.1	10000	20.0	4.654	128.996	1469	375.0	3.919	18960	11331.900	0.1348	14165	1.4165E6	3.411E-3	0.6	2.1
39.000	300.0	4522.9	10000	20.0	4.689	130.000	1474	375.0	3.931	19100	11708.900	0.1358	14636	1.4636E6	3.411E-3	0.7	2.2
40.052	300.0	4509.8	10000	20.0	4.623	131.052	1470	375.0	3.920	18840	11960.300	0.1339	14950	1.4950E6	3.411E-3	0.7	2.2
40.996	300.0	4484.5	10000	20.0	4.639	131.996	1462	375.0	3.897	18900	12212.800	0.1344	15266	1.5266E6	3.411E-3	0.7	2.2
41.996	300.0	4556.9	10000	20.0	4.700	132.996	1485	375.0	3.961	19150	12588.500	0.1362	15736	1.5736E6	3.411E-3	0.7	2.2
42.996	300.0	4506.4	10000	20.0	4.671	133.996	1469	375.0	3.917	19030	12839.800	0.1353	16050	1.6050E6	3.411E-3	0.7	2.2
43.996	300.0	4523.3	10000	20.0	4.672	134.996	1474	375.0	3.932	19040	13218.800	0.1354	16524	1.6524E6	3.411E-3	0.7	2.2
44.996	300.0	4515.1	10000	20.0	4.677	135.996	1472	375.1	3.924	19050	13469.600	0.1355	16837	1.6837E6	3.411E-3	0.7	2.3
46.000	300.0	4482.7	10000	20.0	4.638	137.000	1461	375.0	3.896	18900	13719.700	0.1344	17150	1.7150E6	3.411E-3	0.8	2.3
46.996	300.0	4517.2	10000	20.0	4.664	137.996	1472	375.0	3.926	19000	14096.500	0.1351	17621	1.7621E6	3.411E-3	0.8	2.3
47.996	300.0	4537.1	10000	20.0	4.716	138.996	1479	375.0	3.943	19220	14347.800	0.1366	17935	1.7935E6	3.411E-3	0.8	2.3
48.996	300.0	4535.0	10000	20.0	4.671	139.996	1478	375.0	3.942	19030	14599.100	0.1353	18249	1.8249E6	3.411E-3	0.8	2.3
50.000	300.0	4493.6	10000	20.0	4.629	141.000	1465	375.0	3.906	18860	14977.700	0.1341	18722	1.8722E6	3.411E-3	0.8	2.4
50.996	300.0	4536.4	10000	20.0	4.705	141.996	1479	375.0	3.943	19170	15227.500	0.1363	19034	1.9034E6	3.411E-3	0.8	2.4
51.996	300.0	4502.3	10000	20.0	4.675	142.996	1468	375.0	3.913	19050	15604.600	0.1354	19506	1.9506E6	3.411E-3	0.9	2.4
53.016	300.0	4502.2	10000	20.0	4.645	144.016	1468	375.0	3.914	18930	15855.700	0.1346	19820	1.9820E6	3.411E-3	0.9	2.4
54.008	300.0	4494.1	10000	20.0	4.654	145.008	1465	375.0	3.906	18960	16107.000	0.1348	20134	2.0134E6	3.411E-3	0.9	2.4
55.000	300.0	4512.0	10000	20.0	4.654	146.000	1471	375.0	3.922	18960	16484.199	0.1348	20605	2.0605E6	3.411E-3	0.9	2.4
55.996	300.0	4534.7	10000	20.0	4.663	146.996	1478	375.0	3.941	19000	16735.500	0.1351	20919	2.0919E6	3.411E-3	0.9	2.4
56.996	300.0	4481.5	10000	20.0	4.648	147.996	1461	375.0	3.895	18940	17113.600	0.1347	21392	2.1392E6	3.411E-3	0.9	2.5
57.996	300.0	4520.4	10000	20.0	4.691	148.996	1473	375.0	3.929	19110	17365.000	0.1359	21706	2.1706E6	3.411E-3	1.0	2.5
58.996	300.0	4514.0	10000	20.0	4.622	149.996	1471	375.0	3.924	18830	17615.100	0.1339	22019	2.2019E6	3.411E-3	1.0	2.5
59.996	300.0	4516.8	10000	20.0	4.694	150.996	1472	375.0	3.926	19130	17999.500	0.1360	22499	2.2499E6	3.411E-3	1.0	2.5

Continuous ramp step 2

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0040	296.2	4401.7	10000	20.0	4.742	153.004	1435	370.2	3.875	19320	307.5110	0.1410	384.39	38439	3.411E-3	0.0	2.6
2.0160	292.2	4290.2	10000	20.0	4.761	154.016	1398	365.2	3.829	19400	547.8170	0.1454	684.77	68477	3.411E-3	0.0	2.6
3.0160	288.1	4154.2	10000	20.0	4.800	155.016	1354	360.2	3.760	19560	904.2180	0.1508	1130.3	1.1303E5	3.411E-3	0.1	2.6
4.0160	281.9	3983.0	10000	20.0	4.822	156.016	1298	352.4	3.684	19650	1144.7000	0.1582	1430.9	1.4309E5	3.411E-3	0.1	2.6
5.0200	277.9	3904.5	10000	20.0	4.879	157.020	1273	347.4	3.664	19880	1365.9301	0.1648	1707.4	1.7074E5	3.411E-3	0.1	2.6
6.0160	271.8	3727.6	10000	20.0	4.969	158.016	1215	339.7	3.576	20240	1704.1100	0.1754	2130.1	2.1301E5	3.411E-3	0.1	2.6
7.0200	267.6	3643.4	10000	20.0	4.983	159.020	1188	334.5	3.550	20300	1929.4399	0.1814	2411.8	2.4118E5	3.411E-3	0.1	2.7
8.0160	261.6	3468.9	10000	20.0	5.053	160.016	1131	327.0	3.458	20590	2250.2700	0.1925	2812.8	2.8128E5	3.411E-3	0.1	2.7
9.0160	257.6	3366.7	10000	20.0	5.048	161.016	1097	321.9	3.409	20570	2461.7100	0.1984	3077.1	3.0771E5	3.411E-3	0.2	2.7
10.020	253.4	3263.6	10000	20.0	5.089	162.020	1064	316.8	3.358	20730	2783.2600	0.2066	3479.1	3.4791E5	3.411E-3	0.2	2.7
11.016	247.3	3131.3	10000	20.0	5.170	163.016	1021	309.1	3.302	21060	2981.2500	0.2204	3726.6	3.7266E5	3.411E-3	0.2	2.7
12.016	243.2	3033.6	10000	20.0	5.188	164.016	988.8	304.0	3.252	21140	3181.3601	0.2286	3976.7	3.9767E5	3.411E-3	0.2	2.7
13.016	237.0	2875.6	10000	20.0	5.221	165.016	937.3	296.3	3.163	21270	3481.8501	0.2423	4352.3	4.3523E5	3.411E-3	0.2	2.8
14.016	232.9	2806.4	10000	20.0	5.289	166.016	914.7	291.1	3.142	21550	3675.6899	0.2543	4594.6	4.5946E5	3.411E-3	0.2	2.8
15.028	226.9	2665.1	10000	20.0	5.350	167.028	868.7	283.6	3.063	21800	3958.2700	0.2711	4947.8	4.9478E5	3.411E-3	0.3	2.8
16.016	222.7	2576.1	10000	20.0	5.368	168.016	839.7	278.4	3.016	21870	4145.0898	0.2822	5181.4	5.1814E5	3.411E-3	0.3	2.8
17.016	218.6	2470.1	10000	20.0	5.409	169.016	805.1	273.2	2.947	22040	4327.5601	0.2952	5409.5	5.4095E5	3.411E-3	0.3	2.8
18.016	212.5	2351.6	10000	20.0	5.441	170.016	766.5	265.7	2.885	22170	4589.3398	0.3141	5736.7	5.7367E5	3.411E-3	0.3	2.8
19.020	208.4	2252.2	10000	20.0	5.472	171.020	734.1	260.5	2.818	22290	4764.2598	0.3285	5955.3	5.9553E5	3.411E-3	0.3	2.9
20.020	202.2	2133.8	10000	20.0	5.526	172.020	695.5	252.7	2.752	22520	5021.9502	0.3526	6277.4	6.2774E5	3.411E-3	0.3	2.9
21.016	198.1	2044.3	10000	20.0	5.547	173.016	666.3	247.7	2.691	22600	5183.2900	0.3685	6479.1	6.4791E5	3.411E-3	0.4	2.9
22.016	194.0	1983.9	10000	20.0	5.551	174.016	646.6	242.5	2.666	22620	5345.7402	0.3845	6682.2	6.6822E5	3.411E-3	0.4	2.9
23.000	187.7	1852.4	10000	20.0	5.628	175.000	603.8	234.6	2.573	22930	5589.5298	0.4165	6986.9	6.9869E5	3.411E-3	0.4	2.9
24.016	183.6	1763.6	10000	20.0	5.631	176.016	574.9	229.5	2.504	22940	5746.6401	0.4355	7183.3	7.1833E5	3.411E-3	0.4	2.9
25.020	177.4	1660.1	10000	20.0	5.673	177.020	541.1	221.8	2.440	23110	5964.5601	0.4698	7455.7	7.4557E5	3.411E-3	0.4	3.0
26.016	173.2	1581.3	10000	20.0	5.705	178.016	515.4	216.5	2.381	23240	6114.5801	0.4958	7643.2	7.6432E5	3.411E-3	0.4	3.0
27.016	169.2	1515.2	10000	20.0	5.724	179.016	493.9	211.4	2.336	23320	6252.1699	0.5217	7815.2	7.8152E5	3.411E-3	0.5	3.0
28.016	163.0	1400.7	10000	20.0	5.761	180.016	456.5	203.8	2.241	23470	6458.2100	0.5654	8072.8	8.0728E5	3.411E-3	0.5	3.0
29.016	158.8	1334.8	10000	20.0	5.782	181.016	435.1	198.5	2.192	23560	6595.6099	0.5981	8244.5	8.2445E5	3.411E-3	0.5	3.0
30.020	152.5	1248.4	10000	20.0	5.824	182.020	406.9	190.6	2.135	23730	6789.2100	0.6529	8486.5	8.4865E5	3.411E-3	0.5	3.0
31.016	148.4	1174.8	10000	20.0	5.837	183.016	382.9	185.5	2.064	23780	6914.1401	0.6912	8642.7	8.6427E5	3.411E-3	0.5	3.1
32.016	144.2	1107.2	10000	20.0	5.866	184.016	360.9	180.2	2.002	23900	7038.8301	0.7358	8798.5	8.7985E5	3.411E-3	0.5	3.1
33.016	137.9	1017.5	10000	20.0	5.883	185.016	331.7	172.4	1.923	23970	7213.4902	0.8062	9016.9	9.0169E5	3.411E-3	0.6	3.1
34.016	133.8	961.19	10000	20.0	5.905	186.016	313.3	167.3	1.873	24060	7325.7700	0.8596	9157.2	9.1572E5	3.411E-3	0.6	3.1
35.020	129.6	910.65	10000	20.0	5.919	187.020	296.8	162.0	1.832	24110	7441.0601	0.9184	9301.3	9.3013E5	3.411E-3	0.6	3.1
36.016	123.2	806.29	10000	20.0	5.948	188.016	262.8	153.9	1.707	24230	7600.5898	1.023	9500.7	9.5007E5	3.411E-3	0.6	3.1
37.016	119.1	757.07	10000	20.0	5.965	189.016	246.8	148.8	1.658	24310	7699.9702	1.097	9625.0	9.6250E5	3.411E-3	0.6	3.2
38.016	114.9	705.57	10000	20.0	5.977	190.016	230.0	143.6	1.602	24350	7801.7700	1.181	9752.2	9.7522E5	3.411E-3	0.6	3.2
39.016	108.4	634.14	10000	20.0	5.998	191.016	206.7	135.5	1.526	24440	7942.7900	1.332	9928.5	9.9285E5	3.411E-3	0.7	3.2
40.020	104.3	587.65	10000	20.0	6.013	192.020	191.5	130.4	1.469	24500	8029.9800	1.441	10037	1.0037E6	3.411E-3	0.7	3.2
41.012	100.1	541.33	10000	20.0	6.025	193.012	176.4	125.1	1.410	24550	8118.0000	1.568	10148	1.0148E6	3.411E-3	0.7	3.2
42.020	93.40	472.60	10000	20.0	6.041	194.020	154.0	116.8	1.319	24610	8247.5703	1.806	10309	1.0309E6	3.411E-3	0.7	3.2
43.016	89.20	430.52	10000	20.0	6.055	195.016	140.3	111.5	1.259	24670	8322.1904	1.984	10403	1.0403E6	3.411E-3	0.7	3.3
44.016	84.95	399.93	10000	20.0	6.065	196.016	130.4	106.2	1.228	24710	8396.7500	2.191	10496	1.0496E6	3.411E-3	0.7	3.3
45.020	80.49	359.59	10000	20.0	6.073	197.020	117.2	100.6	1.165	24740	8472.0801	2.444	10590	1.0590E6	3.411E-3	0.8	3.3
46.000	73.93	306.61	10000	20.0	6.090	198.000	99.94	92.41	1.081	24810	8570.3604	2.905	10713	1.0713E6	3.411E-3	0.8	3.3
47.016	69.66	276.41	10000	20.0	6.095	199.016	90.10	87.07	1.035	24840	8632.5596	3.276	10791	1.0791E6	3.411E-3	0.8	3.3
48.016	65.11	242.73	10000	20.0	6.108	200.016	79.12	81.39	0.9721	24880	8694.4102	3.757	10868	1.0868E6	3.411E-3	0.8	3.3
49.000	60.48	215.21	10000	20.0	6.109	201.000	70.15	75.61	0.9278	24890	8774.7500	4.354	10968	1.0968E6	3.411E-3	0.8	3.4
50.020	54.07	176.61	10000	20.0	6.117	202.020	57.57	67.59	0.8517	24920	8823.7695	5.455	11030	1.1030E6	3.411E-3	0.8	3.4
51.016	49.36	150.16	10000	20.0	6.123	203.016	48.95	61.70	0.7933	24950	8872.8896	6.554	11091	1.1091E6	3.411E-3	0.9	3.4
52.016	44.51	126.15	10000	20.0	6.131	204.016	41.12	55.64	0.7390	24980	8915.8398	8.070	11145	1.1145E6	3.411E-3	0.9	3.4
53.016	40.21	106.74	10000	20.0	6.136	205.016	34.79	50.26	0.6922	25000	8952.5801	9.897	11191	1.1191E6	3.411E-3	0.9	3.4
54.020	35.41	83.769	10000	20.0	6.138	206.020	27.30	44.27	0.6168	25010	8989.1299	12.76	11236	1.1236E6	3.411E-3	0.9	3.4
55.020	30.39	64.875	10000	20.0	6.142	207.020	21.15	37.99	0.5566	25030	9019.4502	17.34	11274	1.1274E6	3.411E-3	0.9	3.5
56.016	26.13	49.882	10000	20.0	6.145	208.016	16.26	32.66	0.4978	25040	9043.6602	23.47	11305	1.1305E6	3.411E-3	0.9	3.5
57.012	21.10	35.060	10000	20.0	6.151	209.012	11.43	26.37	0.4334	25060	9067.4199	36.04	11334	1.1334E6	3.411E-3	1.0	3.5
58.012	18.12	26.716	10000	20.0	6.150	210.012	8.708	22.65	0.3844	25060	9090.2695	48.84	11363	1.1363E6	3.411E-3	1.0	3.5
59.016	11.52	12.194	10000	20.0	6.154	211.016	3.975	14.40	0.2760	25070	9095.9199	120.9	11370	1.1370E6	3.411E-3	1.0	3.5
60.020	6.156	3.5374	10000	20.0	6.153	212.020	1.153	7.695	0.1498	25070	9103.9404	423.4	11380	1.1380E6	3.411E-3	1.0	3.5

